Synthesis and Characterization of Iron-Cobalt Nanoparticles
نویسنده
چکیده
Nanoparticles of iron-cobalt have attracted great interest in recent years because of their unique physical and chemical properties because of their industrial importance in preparing magnetic recording materials, pigments, catalysts, etc. With an objective to develop magnetic materials with high saturation magnetization Fe-Co nanosysytems were synthesized by method of chemical reduction reaction of salts aqua-solutions by hydrazine hydrate in alkaline medium. The synthesized powders were characterized by XRD, SEM, EDX and SQUID-magnetometry techniques. The steady-state grain size of 5-20 nm was calculated using XRD line broadening and SEM. The maximum saturation magnetization of 207 and 215 A•m2/kg was achieved at 300 and 5 K, respectively.
منابع مشابه
Cobalt oxide nanoparticles by solid-state thermal decomposition: Synthesis and characterization
In this study, mononuclear octahedral cobalt(III) Schiff base complex [CoL3], L = (5-bromo-2-hydroxybenzyl-2-furylmethyl)imine, was synthesized from the reaction of Co(NO3)2•6H2O and the Schiff base ligand L in methanol as solvent. It used as a new precursor to prepare spinel type cobalt oxide nanoparticles by a facile solid-state thermal decomposition. Controlling the temperature and time, Co3...
متن کاملKCl Promoted Cobalt-iron Nanocatalysts Supported on Silica: Catalytic Performance and Characterization in Fischer-Tropsch Synthesis
The SiO2 supported cobalt-iron nano catalysts were prepared by the sol-gel method. This research investigated the effects of (Co/Fe) wt.%, different Co/Fe ratio at different temperature and loading of KCl wt.% for Fisher-Tropsch synthesis (FTS). The results were showed that the catalyst containing 50 wt.% (Co/Fe)/SiO2 (Co/Fe ratio is 70/30) which promoted with 0.6 wt.% KCl is an optimal nano ca...
متن کاملCobalt(II) macrocycle complexes based synthesis of Co3O4 nanoparticles: structural and spectral characterization
In this paper, macrocyclic cobalt(II) complexes [CoL1](NO3)2.4H2O (1) and [CoL2](NO3)2.2H2O (2) have been synthesized from the reaction of dialdehydes 1,2-bis(2-formylphenyl)ethane and 1,3-bis(2-formylphenyl)propane, Co(NO3)2.6H2O and 1,2-cyclohexanediamine with molar ration 1:1:1 in methanole and characterized by elemental analyses and FT-IR spectroscopy. Then used as precursors for preparatio...
متن کاملSynthesis and Characterization of Iron Oxide Nanoparticles by Thermal Decomposition Method of Iron (III) Chelates
Magnetic iron oxide nanoparticles have numerous applications in the biomedical field. This paper reports the preparation and properties of iron oxide nanoparticles synthesised by thermal decomposition method from iron chelates. The iron oxide nanoparticles were characterized by FTIR, powder XRD, VSM, SEM and TEM techniques. FTIR and powder XRD studies show that iron oxide was fo...
متن کاملFabrication and Characterization of Nanoporous Co Oxide (Co3O4) Prepared by Simple Sol-gel Synthesis
Cobalt oxide (Co3O4) nanorods were prepared by a simple co-precipitation method using ethanol solution of cobalt nitrate as precursor and cetyl trimethylammonium bromide (CTAB) as surfactant. Morphological properties of the nanoparticles were characterized. XRD measurement exhibited the structure of Co3O4 nanocrystals for annealed samples. The SEM ima...
متن کاملRoom Temperature Ferromagnetism in Cobalt Doped ZnO Nanoparticles
In this work we report synthesis and magnetic characterization of cobalt doped ZnO nanoparticles (with different percent of doped cobalt oxide). Synthesis of the materials was carried out at room temperature by polyacrylamide-gel method, using zink sulfate and cobalt nitrate as source materials, acrylamide as monomer and N,N-methylene bisacrylamide as a lattice reagent. Characterization of the ...
متن کامل